TY  - SER
AU  - Grebennikov,Andrei V.
AU  - Kuzmin,Yaroslav V.
AU  - Glascock,Michael D.
AU  - Wada,Keiji
AU  - Ferguson,Jeffrey R.
AU  - Kim,Jong Chan
AU  - Popov,Vladimir K.
AU  - Rasskazov,Sergei V.
AU  - Yasnygina,Tatyana A.
AU  - Saito,Noriyuki
AU  - Takehara,Hironobu
AU  - Carter,Tristan
AU  - Kasztovszky,Zsolt
AU  - Biró,Katalin T.
AU  - Ono,Akira
AU  - Suda,Yoshimitsu
TI  - Inter-laboratory validation of the WDXRF, EDXRF, ICP–MS, NAA and PGAA analytical techniques and geochemical characterisation of obsidian sources in northeast Hokkaido Island, Japan
KW  - обсидиан
KW  - геохимическая характеристика
KW  - Хоккайдо, остров
KW  - рентгеновская флуоресценция
KW  - масс-спектрометрия с индуктивно-связанной плазмой
KW  - нейтронно-активационный анализ
KW  - гамма-активационный анализ
KW  - статьи в журналах
N1  - Библиогр.: с. 392
N2  - Obsidian provenance studies, based on geochemical signatures, are important for determining the source regions of obsidian artefacts. Such research depends on the availability of reproducible geochemical data. An interlaboratory study was conducted to validate analytical methods applied to samples from four obsidian sources in northeast Hokkaido Island (Shirataki, Rubeshibe, and Oketo regions). The methods applied were WavelengthDispersive X-ray Fluorescence (WDXRF), Energy-Dispersive X-ray Fluorescence (EDXRF), Inductively Coupled Plasma–Mass Spectrometry (ICP–MS), Neutron Activation Analysis (NAA) and Prompt-Gamma Activation Analysis (PGAA). Eight laboratories in Japan, the Russian Federation, Republic Korea, Hungary, Canada, and the USA took part in the trials. Results indicate discrepancies between laboratories, but compositional data for 53 elements were successfully compiled, and reference compositions for 16 elements in each sample defined. Based on these data, a new chemical discrimination scheme is proposed for obsidian sources in the Shirataki, Rubeshibe, and Oketo regions. This scheme is applicable to the discrimination of obsidian sources using semiquantitative EDXRF analysis, with this being important in non-destructive provenance studies of artefacts. This study fosters the further establishment of reference materials for obsidian sources in the Hokkaido region, and the sharing of such materials
UR  - http://vital.lib.tsu.ru/vital/access/manager/Repository/vtls:000673067
ER  -